Structures by: Das K.

Total: 55

C14H11CoN9

C14H11CoN9

Pal, PampiKonar, SaugataLama, PremDas, KinsukBauzá, AntonioFrontera, AntonioMukhopadhyay, Subrata

The journal of physical chemistry. B (2016) 120, 27 6803-6811

a=13.9366(10)Å   b=8.8995(6)Å   c=14.6385(10)Å

α=90.00°   β=117.760(2)°   γ=90.00°

C10H14CoN8O2

C10H14CoN8O2

Pal, PampiKonar, SaugataLama, PremDas, KinsukBauzá, AntonioFrontera, AntonioMukhopadhyay, Subrata

The journal of physical chemistry. B (2016) 120, 27 6803-6811

a=6.4415(5)Å   b=7.3787(6)Å   c=8.5998(8)Å

α=105.661(4)°   β=107.985(3)°   γ=96.254(3)°

C38H34Cd2Cl2N12O10

C38H34Cd2Cl2N12O10

Jana, AtanuSukul, Pradip K.Mandal, Sushil K.Konar, SaugataRay, SangitaDas, KinsukGolen, James A.Rheingold, Arnold L.Mondal, SudipaMondal, Tapan K.Khuda-Bukhsh, Anisur RKar, Susanta K.

The Analyst (2014) 139, 2 495-504

a=23.0762(15)Å   b=12.6124(6)Å   c=17.5274(13)Å

α=90.00°   β=116.6010(10)°   γ=90.00°

C26H22Cl2Cu2N8O6

C26H22Cl2Cu2N8O6

Saugata KonarAtanu JanaKinsuk DasSangita RaySudipta ChatterjeeSusanta Kumar Kar

Inorganica Chimica Acta (2013) 395, 1-10

a=16.524(4)Å   b=7.958(2)Å   c=21.913(4)Å

α=90.00°   β=90.00°   γ=90.00°

C18H14ClCuN5O7

C18H14ClCuN5O7

Saugata KonarAtanu JanaKinsuk DasSangita RaySudipta ChatterjeeSusanta Kumar Kar

Inorganica Chimica Acta (2013) 395, 1-10

a=14.611(6)Å   b=15.551(6)Å   c=8.837(4)Å

α=90.00°   β=102.36(1)°   γ=90.00°

C14H14N4O3

C14H14N4O3

Saugata KonarAtanu JanaKinsuk DasSangita RaySudipta ChatterjeeSusanta Kumar Kar

Inorganica Chimica Acta (2013) 395, 1-10

a=9.2653(4)Å   b=12.7937(6)Å   c=12.3970(5)Å

α=90.00°   β=97.675(2)°   γ=90.00°

C13H13ClCuN4O8,H2O

C13H13ClCuN4O8,H2O

Saugata KonarAtanu JanaKinsuk DasSangita RaySudipta ChatterjeeSusanta Kumar Kar

Inorganica Chimica Acta (2013) 395, 1-10

a=12.6415(16)Å   b=21.044(3)Å   c=28.970(4)Å

α=90.00°   β=90.00°   γ=90.00°

C18H14CuN6O6

C18H14CuN6O6

Saugata KonarAtanu JanaKinsuk DasSangita RaySudipta ChatterjeeSusanta Kumar Kar

Inorganica Chimica Acta (2013) 395, 1-10

a=15.0825(6)Å   b=8.2354(3)Å   c=15.4752(7)Å

α=90.00°   β=107.587(2)°   γ=90.00°

C22H26Cl2N12O11Zn

C22H26Cl2N12O11Zn

Saugata KonarAtanu JanaKinsuk DasSangita RayJames A. GolenArnold L. RheingoldSusanta Kumar Kar

Inorganica Chimica Acta (2013) 397, 144-151

a=11.4714(14)Å   b=12.0739(14)Å   c=13.8484(17)Å

α=95.2900(10)°   β=96.499(2)°   γ=108.4850(10)°

C22H30Cl2N14O12Zn

C22H30Cl2N14O12Zn

Saugata KonarAtanu JanaKinsuk DasSangita RayJames A. GolenArnold L. RheingoldSusanta Kumar Kar

Inorganica Chimica Acta (2013) 397, 144-151

a=11.7107(6)Å   b=12.0150(6)Å   c=12.1097(6)Å

α=101.5930(10)°   β=97.9330(10)°   γ=94.9240(10)°

C68H76.75Cd5Cl4N36O29.5

C68H76.75Cd5Cl4N36O29.5

Saugata KonarAtanu JanaKinsuk DasSangita RayJames A. GolenArnold L. RheingoldSusanta Kumar Kar

Inorganica Chimica Acta (2013) 397, 144-151

a=45.815(12)Å   b=13.880(3)Å   c=16.375(4)Å

α=90.00°   β=106.948(6)°   γ=90.00°

C26H18N4O6Pb

C26H18N4O6Pb

Paul, AnupDas, KabitaKarmakar, AnirbanGuedes da Silva, M Fátima CPombeiro, Armando J. L.

Dalton transactions (Cambridge, England : 2003) (2020) 49, 37 12970-12984

a=17.1194(13)Å   b=5.1144(3)Å   c=25.2616(15)Å

α=90°   β=92.795(4)°   γ=90°

C20H20N3O7Zn

C20H20N3O7Zn

Paul, AnupDas, KabitaKarmakar, AnirbanGuedes da Silva, M Fátima CPombeiro, Armando J. L.

Dalton transactions (Cambridge, England : 2003) (2020) 49, 37 12970-12984

a=8.554(3)Å   b=11.089(4)Å   c=11.895(4)Å

α=90.098(9)°   β=110.130(12)°   γ=90.113(9)°

C26H22CdN4O8

C26H22CdN4O8

Paul, AnupDas, KabitaKarmakar, AnirbanGuedes da Silva, M Fátima CPombeiro, Armando J. L.

Dalton transactions (Cambridge, England : 2003) (2020) 49, 37 12970-12984

a=7.7745(5)Å   b=8.7385(6)Å   c=10.6928(7)Å

α=105.022(2)°   β=95.322(3)°   γ=116.297(2)°

[(Bim2NNN)RuCl(PPh3)2]PF6

C55H43ClF6N5P3Ru

Dutta, MoumitaDas, KanuPrathapa, Siriyara JagannathaSrivastava, Hemant KumarKumar, Akshai

Chemical communications (Cambridge, England) (2020) 56, 68 9886-9889

a=9.9974(5)Å   b=38.806(4)Å   c=13.9459(7)Å

α=90°   β=92.722(5)°   γ=90°

(tBu2NNN)RuCl2(PPh3)

C35H42Cl6N3PRu

Dutta, MoumitaDas, KanuPrathapa, Siriyara JagannathaSrivastava, Hemant KumarKumar, Akshai

Chemical communications (Cambridge, England) (2020) 56, 68 9886-9889

a=16.093(4)Å   b=20.363(5)Å   c=23.088(6)Å

α=90°   β=90°   γ=90°

C18H18BrMnN2O3S

C18H18BrMnN2O3S

Das, KalicharanMondal, AvijitSrimani, Dipankar

Chemical communications (Cambridge, England) (2018) 54, 75 10582-10585

a=16.5242(15)Å   b=9.5030(8)Å   c=26.035(3)Å

α=90.00°   β=90.00°   γ=90.00°

C15H15ClN3NiO2,Cl

C15H15ClN3NiO2,Cl

Pal, PampiDas, KinsukHossain, AnowarFrontera, AntonioMukhopadhyay, Subrata

New Journal of Chemistry (2020) 44, 18 7310-7318

a=12.485(6)Å   b=9.687(4)Å   c=14.318(6)Å

α=90°   β=105.290(15)°   γ=90°

C15H11Cl2CuN3

C15H11Cl2CuN3

Pal, PampiDas, KinsukHossain, AnowarFrontera, AntonioMukhopadhyay, Subrata

New Journal of Chemistry (2020) 44, 18 7310-7318

a=10.6709(10)Å   b=8.2581(7)Å   c=16.0905(16)Å

α=90°   β=94.686(3)°   γ=90°

C52H94N8NiO8

C52H94N8NiO8

Das, KuheliBeyene, Belete B.Datta, AmitabhaGarribba, EugenioRoma-Rodrigues, CatarinaSilva, AnaFernandes, Alexandra R.Hung, Chen-Hsiung

New Journal of Chemistry (2018) 42, 11 9126

a=20.3385(7)Å   b=17.4098(6)Å   c=18.5302(6)Å

α=90°   β=117.635(2)°   γ=90°

C51H96MnN8O10

C51H96MnN8O10

Das, KuheliBeyene, Belete B.Datta, AmitabhaGarribba, EugenioRoma-Rodrigues, CatarinaSilva, AnaFernandes, Alexandra R.Hung, Chen-Hsiung

New Journal of Chemistry (2018) 42, 11 9126

a=11.7263(4)Å   b=16.4104(6)Å   c=17.1352(6)Å

α=66.452(2)°   β=79.714(2)°   γ=79.713(2)°

C12H11NO2

C12H11NO2

Jain, KavitaChaudhuri, SaikatPal, KuntalDas, Kalpataru

New Journal of Chemistry (2019) 43, 3 1299

a=7.4403(5)Å   b=7.5372(5)Å   c=10.8823(7)Å

α=100.819(2)°   β=96.705(2)°   γ=113.4590(10)°

(C69H51Eu2N12O9),8(H2O)

(C69H51Eu2N12O9),8(H2O)

Das, KuheliNandi, SoumendraMondal, SudipaAskun, TulinCantürk, ZerrinCelikboyun, PinarMassera, ChiaraGarribba, EugenioDatta, AmitabhaSinha, ChittaranjanAkitsu, Takashiro

New J. Chem. (2015) 39, 2 1101

a=46.333(3)Å   b=17.2990(10)Å   c=32.343(2)Å

α=90.00°   β=123.5420(10)°   γ=90.00°

C21H19CuN3O5

C21H19CuN3O5

Das, KuheliPanda, UttamDatta, AmitabhaRoy, SumanMondal, SudipaMassera, ChiaraAskun, TulinCelikboyun, PinarGarribba, EugenioSinha, ChittaranjanAnand, KushiAkitsu, TakashiroKobayashi, Kana

New J. Chem. (2015) 39, 9 7309

a=8.2580(10)Å   b=11.221(2)Å   c=21.508(3)Å

α=90.00°   β=97.190(2)°   γ=90.00°

'C34H32Cu3N6O10

'C34H32Cu3N6O10

Datta, AmitabhaDas, KuheliMane, Sandeep B.Mendiratta, ShrutiEl Fallah, Mohamed SalahGarribba, EugenioBauzá, AntonioFrontera, AntonioHung, Chen-HsiungSinha, Chittaranjan

RSC Advances (2016) 6, 60 54856

a=8.8854(4)Å   b=11.6472(5)Å   c=16.0930(6)Å

α=90°   β=101.034(2)°   γ=90°

2(C12H11Cu1N3O4),H2O

2(C12H11Cu1N3O4),H2O

Pal, PampiKonar, SaugataEl Fallah, Mohamed SalahDas, KinsukBauzá, AntonioFrontera, AntonioMukhopadhyay, Subrata

RSC Advances (2015) 5, 56 45082-45091

a=20.402(5)Å   b=7.233(5)Å   c=18.215(5)Å

α=90.000°   β=112.363(5)°   γ=90.000°

C10H11CuN5O6

C10H11CuN5O6

Pal, PampiKonar, SaugataEl Fallah, Mohamed SalahDas, KinsukBauzá, AntonioFrontera, AntonioMukhopadhyay, Subrata

RSC Advances (2015) 5, 56 45082-45091

a=7.3423(3)Å   b=8.8649(4)Å   c=11.4482(5)Å

α=89.440(4)°   β=80.271(3)°   γ=67.287(3)°

C37H35Cl2NPRuS2

C37H35Cl2NPRuS2

Biswas, NanditaDas, KalicharanSardar, BitanSrimani, Dipankar

Dalton transactions (Cambridge, England : 2003) (2019) 48, 19 6501-6512

a=9.7186(6)Å   b=11.8743(7)Å   c=18.0974(11)Å

α=71.496(4)°   β=79.588(4)°   γ=79.316(4)°

C31H36Cl2NPRuS2

C31H36Cl2NPRuS2

Biswas, NanditaDas, KalicharanSardar, BitanSrimani, Dipankar

Dalton transactions (Cambridge, England : 2003) (2019) 48, 19 6501-6512

a=10.7565(6)Å   b=12.0194(7)Å   c=12.7360(8)Å

α=90.215(5)°   β=92.041(5)°   γ=107.252(5)°

C44H44Cl2Cu4N24O12,2(ClO4)

C44H44Cl2Cu4N24O12,2(ClO4)

Mandal, Tarak NathRoy, SomnathKonar, SaugataJana, AtanuRay, SangitaDas, KinsukSaha, RajatEl Fallah, Mohamed SalahButcher, Ray J.Chatterjee, SudiptaKar, Susanta Kumar

Dalton transactions (Cambridge, England : 2003) (2011) 40, 44 11866-11875

a=14.745(1)Å   b=21.597(1)Å   c=26.180(2)Å

α=90.00°   β=121.57(1)°   γ=90.00°

C64H56N28Ni4O4,4(NO3),4(H2O),2(C2N),4(O)

C64H56N28Ni4O4,4(NO3),4(H2O),2(C2N),4(O)

Mandal, Tarak NathRoy, SomnathKonar, SaugataJana, AtanuRay, SangitaDas, KinsukSaha, RajatEl Fallah, Mohamed SalahButcher, Ray J.Chatterjee, SudiptaKar, Susanta Kumar

Dalton transactions (Cambridge, England : 2003) (2011) 40, 44 11866-11875

a=14.105(9)Å   b=14.105(9)Å   c=38.379(4)Å

α=90.00°   β=90.00°   γ=90.00°

C19H24Cu2N10O12

C19H24Cu2N10O12

Mandal, Tarak NathRoy, SomnathKonar, SaugataJana, AtanuRay, SangitaDas, KinsukSaha, RajatEl Fallah, Mohamed SalahButcher, Ray J.Chatterjee, SudiptaKar, Susanta Kumar

Dalton transactions (Cambridge, England : 2003) (2011) 40, 44 11866-11875

a=8.8162(4)Å   b=10.2990(5)Å   c=16.3062(5)Å

α=74.779(3)°   β=88.629(3)°   γ=65.135(4)°

C64H56Cu4N28O4,4(NO3)

C64H56Cu4N28O4,4(NO3)

Mandal, Tarak NathRoy, SomnathKonar, SaugataJana, AtanuRay, SangitaDas, KinsukSaha, RajatEl Fallah, Mohamed SalahButcher, Ray J.Chatterjee, SudiptaKar, Susanta Kumar

Dalton transactions (Cambridge, England : 2003) (2011) 40, 44 11866-11875

a=19.921(7)Å   b=38.224(16)Å   c=14.084(5)Å

α=90.00°   β=134.890(5)°   γ=90.00°

C72H72Mn5N30O6,4(ClO4),(H2O)

C72H72Mn5N30O6,4(ClO4),(H2O)

Mandal, T. N.Roy, S.Konar, S.Jana, A.Das, K.Ray, S.Gupta, S.Saha, R.El Fallah, M. S.Tercero, J.Butcher, R. J.Chatterjee, S.Kar, S. K.

Dalton transactions (Cambridge, England : 2003) (2012) 41, 2 413-423

a=13.832(6)Å   b=14.491(6)Å   c=25.245(11)Å

α=89.257(6)°   β=88.790(6)°   γ=61.571(5)°

C90H78Mn5N48O6,4(ClO4),3(H2O)

C90H78Mn5N48O6,4(ClO4),3(H2O)

Mandal, T. N.Roy, S.Konar, S.Jana, A.Das, K.Ray, S.Gupta, S.Saha, R.El Fallah, M. S.Tercero, J.Butcher, R. J.Chatterjee, S.Kar, S. K.

Dalton transactions (Cambridge, England : 2003) (2012) 41, 2 413-423

a=15.011(2)Å   b=28.447(4)Å   c=26.921(3)Å

α=90.00°   β=107.93(1)°   γ=90.00°

C38H40Cu2N4Na2O10,2(ClO4),H2O

C38H40Cu2N4Na2O10,2(ClO4),H2O

Datta, AmitabhaDas, KuheliMassera, ChiaraClegg, Jack K.Sinha, ChittaranjanHuang, Jui-HsienGarribba, Eugenio

Dalton transactions (Cambridge, England : 2003) (2014) 43, 14 5558-5563

a=9.7605(2)Å   b=17.0778(3)Å   c=12.4657(3)Å

α=90.00°   β=94.379(2)°   γ=90.00°

(Cy2NNN)RuCl2(CO)

C43H64Cl4N6O5Ru2

Das, KanuYasmin, EileenDas, BabulalSrivastava, Hemant KumarKumar, Akshai

Catalysis Science & Technology (2020) 10, 24 8347-8358

a=12.5519(9)Å   b=23.6646(18)Å   c=16.9746(12)Å

α=90.00°   β=94.020(2)°   γ=90.00°

(iPr2NNN)RuCl2(CO)

C14H21Cl2N3O2Ru

Das, KanuYasmin, EileenDas, BabulalSrivastava, Hemant KumarKumar, Akshai

Catalysis Science & Technology (2020) 10, 24 8347-8358

a=9.2304(5)Å   b=10.8098(6)Å   c=18.2395(11)Å

α=90.00°   β=96.278(2)°   γ=90.00°

2(C7H3Fe2O6Te1),C1H2Te2

2(C7H3Fe2O6Te1),C1H2Te2

Das, K.Sinha, U. C.Mathur, P.

Acta Crystallographica Section C (1992) 48, 8 1386-1389

a=28.865(10)Å   b=13.787(7)Å   c=14.733(4)Å

α=90°   β=104.67(2)°   γ=90°

2(C7H3Fe2O6Te1),C1H2Te2

2(C7H3Fe2O6Te1),C1H2Te2

Das, K.Sinha, U. C.Mathur, P.

Acta Crystallographica Section C (1992) 48, 8 1386-1389

a=28.865(10)Å   b=13.787(7)Å   c=14.733(4)Å

α=90°   β=104.67(2)°   γ=90°

C6H11O6,C6H4,I

C6H11O6,C6H4,I

Banerjee, R.Das, K.Ganesh, V.Banerjee, P.Surolia, A.Vijayan, M.

Acta Crystallographica Section C (1994) 50, 11 1726-1728

a=10.049(2)Å   b=4.6790(10)Å   c=14.4290(10)Å

α=90.°   β=107.28(3)°   γ=90.°

Di-μ-azido-bis({<i>N</i>-[1-(2-pyridyl- κ<i>N</i>)ethylidene]acetohydrazidato-κ^2^<i>N</i>',<i>O</i>}dicopper(II))

C18H20Cu2N12O2

Datta, AmitabhaDas, KuheliJhou, Yan-MingHuang, Jui-HsienLee, Hon Man

Acta Crystallographica Section E (2010) 66, 10 m1271

a=7.589(3)Å   b=8.955(3)Å   c=9.693(4)Å

α=66.534(15)°   β=69.461(13)°   γ=81.468(16)°

Dichlorido{<i>N</i>-[1-(2-pyridin-2-yl)ethylidene]acetohydrazide- κ^2^<i>N</i>',<i>O</i>}copper(II)

C9H11Cl2CuN3O

Datta, AmitabhaDas, KuheliJhou, Yan-MingHuang, Jui-HsienLee, Hon Man

Acta Crystallographica Section E (2011) 67, 1 m123

a=6.6501(15)Å   b=15.680(3)Å   c=13.103(2)Å

α=90.00°   β=118.769(12)°   γ=90.00°

C14H12BrMnN2O3S

C14H12BrMnN2O3S

Jana, AkashDas, KuhaliKundu, AbhishekThorve, Pradip RamdasAdhikari, DebashisMaji, Biplab

ACS Catalysis (2020) 2615

a=7.5394(3)Å   b=9.7257(4)Å   c=11.6722(5)Å

α=108.970(4)°   β=99.234(3)°   γ=101.738(3)°

C15H14BrMnN2O3S

C15H14BrMnN2O3S

Jana, AkashDas, KuhaliKundu, AbhishekThorve, Pradip RamdasAdhikari, DebashisMaji, Biplab

ACS Catalysis (2020) 2615

a=6.6200(3)Å   b=7.8565(5)Å   c=17.0496(7)Å

α=83.308(4)°   β=86.928(4)°   γ=73.022(5)°

C13H16BrMnN2O3S

C13H16BrMnN2O3S

Das, KalicharanMondal, AvijitSrimani, Dipankar

The Journal of organic chemistry (2018) 83, 16 9553-9560

a=7.9663(16)Å   b=14.830(3)Å   c=14.187(2)Å

α=90.00°   β=96.629(18)°   γ=90.00°

C23H23NO3S

C23H23NO3S

Manas K. GhoraiDipti ShuklaKalpataru Das

Journal of Organic Chemistry (2009) 74, 7013-7022

a=8.508(5)Å   b=10.467(5)Å   c=22.375(5)Å

α=90.00°   β=90.00°   γ=90.00°

C23H23NO3S

C23H23NO3S

Manas K. GhoraiDipti ShuklaKalpataru Das

Journal of Organic Chemistry (2009) 74, 7013-7022

a=9.986(5)Å   b=19.659(5)Å   c=20.658(5)Å

α=90.00°   β=90.00°   γ=90.00°

C48H62Br2S5

C48H62Br2S5

Andrzej RajcaMaren PinkShuzhang XiaoMakoto MiyasakaSuchada RajcaKausik DasKristin Plessel

Journal of Organic Chemistry (2009) 74, 7504-7513

a=9.9503(11)Å   b=12.8178(15)Å   c=18.659(2)Å

α=86.056(3)°   β=78.703(3)°   γ=80.682(3)°

C24H32Br2S2

C24H32Br2S2

Andrzej RajcaMaren PinkShuzhang XiaoMakoto MiyasakaSuchada RajcaKausik DasKristin Plessel

Journal of Organic Chemistry (2009) 74, 7504-7513

a=14.6460(12)Å   b=4.7274(4)Å   c=18.0088(14)Å

α=90.00°   β=104.994(2)°   γ=90.00°

C32H29Cl2N2PRuS

C32H29Cl2N2PRuS

Biswas, NanditaDas, KalicharanSardar, BitanSrimani, Dipankar

Dalton transactions (Cambridge, England : 2003) (2019) 48, 19 6501-6512

a=10.1370(4)Å   b=11.4066(4)Å   c=16.0632(6)Å

α=73.196(2)°   β=80.920(2)°   γ=67.294(2)°

C66H66Mn5N36O6,4(ClO4),4(H2O)

C66H66Mn5N36O6,4(ClO4),4(H2O)

Mandal, T. N.Roy, S.Konar, S.Jana, A.Das, K.Ray, S.Gupta, S.Saha, R.El Fallah, M. S.Tercero, J.Butcher, R. J.Chatterjee, S.Kar, S. K.

Dalton transactions (Cambridge, England : 2003) (2012) 41, 2 413-423

a=34.1672(11)Å   b=19.6474(7)Å   c=29.3633(9)Å

α=90.00°   β=111.754(2)°   γ=90.00°

(C24H34N7O6Ni2),(Cl1O4),2(H2O)

(C24H34N7O6Ni2),(Cl1O4),2(H2O)

Das, KuheliDatta, AmitabhaNandi, SoumendranathMane, Sandeep B.Mondal, SudipaMassera, ChiaraSinha, ChittaranjanHung, Chen-HsiungAskun, TulinCelikboyun, PinarCantürk, ZerrinGarribba, EugenioAkitsu, Takashiro

Inorganic Chemistry Frontiers (2015) 2, 8 749

a=11.748(2)Å   b=11.0930(10)Å   c=13.278(2)Å

α=90.000(5)°   β=100.963(2)°   γ=90.000(5)°

C68H66Co3N8O16S2

C68H66Co3N8O16S2

Datta, AmitabhaDas, KuheliMassera, ChiaraClegg, Jack K.Pfrunder, Michael C.Garribba, EugenioHuang, Jui-HsienSinha, ChittaranjanMaji, Tapas KumarAkitsu, TakashiroOrita, Shingo

Inorganic Chemistry Frontiers (2015) 2, 2 157

a=10.616(5)Å   b=11.949(4)Å   c=14.908(6)Å

α=80.973(6)°   β=83.402(6)°   γ=73.213(5)°

C34H31Co1.50N4O7S

C34H31Co1.50N4O7S

Datta, AmitabhaDas, KuheliMassera, ChiaraClegg, Jack K.Pfrunder, Michael C.Garribba, EugenioHuang, Jui-HsienSinha, ChittaranjanMaji, Tapas KumarAkitsu, TakashiroOrita, Shingo

Inorganic Chemistry Frontiers (2015) 2, 2 157

a=10.6094(6)Å   b=11.9098(6)Å   c=14.7412(7)Å

α=81.495(4)°   β=83.114(4)°   γ=72.479(5)°